Glomeration and was previouslywas previously reported that of a polysaccharide can
Glomeration and was previouslywas previously reported that of a polysaccharide might be increased by in- be improved by reported that the aggregation the aggregation of a polysaccharide can introducing (for example, sulfate groups) that enhance its inter and enhance its inter and troducing functional groupsfunctional groups (for example, sulfate groups) that intraintramolecular interactions or polyelectrolyte effects [602]. Therefore, the results obtained in molecular interactions or polyelectrolyte effects [602]. Hence, the outcomes obtained in our our perform correspond to perform correspond for the literary sources.the literary sources.1abFigure 9. Cont.cFoods 2021, 10,12 ofc021, 10, x FOR PEER REVIEW13 ofdFigure 9. AFM data xanthan and (two) xanthan sulfate (relief sulfate (relief (a), (b), 3D relief (c), and particle size Figure 9. AFM data on (1) initial on (1) initial xanthan and (2) xanthan (a), phase contrastphase contrast (b), 3D relief (c), and particle size distribution (d)). distribution (d)).In accordance with the ML-SA1 TRP Channel phase-contrastphase-contrast information (Figure 9b),the films of thethe films on the initial In accordance with the information (Figure 9b), the surface on the surface of initial and sulfated xanthan gum does not include impurities. and sulfated xanthan gum will not contain impurities. The particle size distribution distribution (Figure 9d) has of aform of a distribution The particle size (Figure 9d) has the kind the typical typical distribution (Gaus(Gaussian distribution), each for the original and for sulfated sulfated xanthan. sian distribution), each for the original and for xanthan. The embedding of embedding of a into a xanthaninto a xanthan moleculemolecular its molecular The a sulfate group sulfate group molecule decreases its decreases weight as well as leads as well as leads in amorphism in amorphism and aggregation. weight to an increase to an increase and aggregation. four. Conclusions4. ConclusionsIn proposed a new approach for strategy for the xanthan Tenidap Immunology/Inflammation polysacchaIn this function, we this perform, we proposed a new the synthesis ofsynthesis of xanthan polysaccharides making use of acid upon activation with urea derivatives. It has It has been shown rides applying sulfamic sulfamic acid upon activation with urea derivatives. been shown that that urea has the highest activating activity inside the reaction of sulfation of xanthan with urea has the highest activating activity within the reaction of sulfation of xanthan with sulfamic sulfamic acid. The influence on the of your sulfating complicated, the temperature, and also the du-the duration of acid. The influence on the amount amount of the sulfating complex, the temperature, and also the sulfation method around the sulfur content in xanthan sulfate has been established. It has ration from the sulfation procedure around the sulfur content in xanthan sulfate has been estabbeen shown that the optimal conditions for xanthan sulfation are: the amount lished. It has been shown that the optimal situations for xanthan sulfation are: the amount of sulfating complex per 1 g xanthan is 3.5 mmol, the temperature is 90 , along with the of sulfating complicated per 1 g of of xanthan is three.five mmol, the temperature is 90 C, plus the duration is duration is two.three two.3 h. reaction item with all the maximum sulfur contentcontent was analyzed by FTIR h. The The reaction solution together with the maximum sulfur was analyzed by spectroscopy, X-ray diffraction, gel penetration microscopy, thermal evaluation, and atomic FTIR spectroscopy, X-ray diffraction, gel penetration microscopy, thermal evaluation, a.